process equipment

Crystallizer

Controlled crystal size from process to product — FC, DTB, and Oslo configurations.

Ermak Proses crystallizers are engineered for consistent crystal size distribution and high product purity. Three configuration options — forced circulation (FC), draft-tube baffle (DTB), and Oslo-type — cover the full range of industrial crystallization requirements, from bulk chemical salts to pharmaceutical intermediates.

Crystallizer — Controlled crystal size from process to product — FC, DTB, and Oslo configurations.

How Industrial Crystallizers Work

Crystallization is the process of forming solid crystals from a solution, melt, or gas. In industrial crystallizers, the driving force is supersaturation — the condition where the solution contains more dissolved solid than it can hold at equilibrium. Supersaturation is achieved by evaporating solvent, cooling the solution, or adding an anti-solvent.

Once supersaturation is reached, nucleation begins: tiny crystal nuclei form spontaneously or on seed crystals. These nuclei then grow by deposition of dissolved material onto their surfaces. The key engineering challenge is controlling the balance between nucleation rate and crystal growth rate to achieve the target crystal size distribution (CSD).

The three Ermak Proses crystallizer types address this control challenge differently. Forced circulation (FC) crystallizers use a high-velocity pump circuit to maintain supersaturation uniformly throughout the vessel. DTB crystallizers use an internal draft tube to create controlled upflow and a baffle to separate fine crystals for dissolution, producing narrower CSD. Oslo-type crystallizers maintain a fluidized crystal bed in the growth zone with feed entering below the bed, enabling the largest and most uniform crystals.

Quick Reference

Crystallizer typeFC (Forced Circulation), DTB (Draft Tube Baffle), Oslo
Operating modeContinuous or batch
Crystal size range (typical)100 µm – 5 mm (product-dependent)
Supersaturation controlEvaporation-based, cooling-based, or combined
Operating temperature0°C – 200°C (application-dependent)
Operating pressureVacuum to 6 bar (g)
Materials of constructionSS 304, SS 316L, Duplex, Hastelloy (product-dependent)
Full specifications ↓

Technical Specifications

All parameters are indicative ranges. Final sizing is determined by process simulation based on your specific material and throughput requirements.

Standard Operating Parameters

ParameterValue / Range
Crystallizer typeFC (Forced Circulation), DTB (Draft Tube Baffle), Oslo
Operating modeContinuous or batch
Crystal size range (typical)100 µm – 5 mm (product-dependent)
Supersaturation controlEvaporation-based, cooling-based, or combined
Operating temperature0°C – 200°C (application-dependent)
Operating pressureVacuum to 6 bar (g)
Materials of constructionSS 304, SS 316L, Duplex, Hastelloy (product-dependent)
Capacity range500 kg/h – 50 t/h crystalline product

Configuration Comparison

ParameterValue / Range
Forced Circulation (FC)Wide CSD, handles scaling, broad application range, lowest capex
Draft Tube Baffle (DTB)Narrow CSD, high purity, fine crystal removal, mid-range capex
Oslo typeLargest crystals, fluidized bed growth zone, highest product uniformity

Need a technical pre-sizing? Send us your material data sheet, moisture content, required throughput and energy source — we return a technical sizing with drum dimensions and energy balance within 2 business days.

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Typical Crystallization Applications

Reference data from industrial installations. Actual values depend on feed consistency, particle size distribution and required product quality.

MaterialInlet moistureOutlet moistureParticle sizeGas temp.Industry
Sodium chloride (NaCl)Saturated brine< 0.1% moisture0.5–3 mm80–110°CChemical / Food
Ammonium sulfate ((NH₄)₂SO₄)Process liquor< 0.5%1–4 mm50–80°CFertilizer
Citric acidFermentation broth< 0.2%0.3–1.5 mm20–40°CFood / Pharma
Lithium carbonate (Li₂CO₃)Leach liquor< 0.1%0.5–2 mm60–90°CMining / Battery

Don't see your material? Send us your process data and we'll provide material-specific sizing.

Crystallizer Types

1

Forced Circulation (FC) Crystallizer

Saturated solution is continuously circulated at high velocity through the vessel and an external heat exchanger. The heat exchanger generates the supersaturation by evaporation (vacuum) or cooling. Robust against scaling due to high wall velocity.

Best for:Salts, ammonium sulfate, sodium chloride, broad range of inorganic chemicals
2

Draft Tube Baffle (DTB) Crystallizer

An internal draft tube creates an upward flow in the centre of the vessel; a baffle around the draft tube creates a clarified zone where fine crystals are separated and returned for dissolution. This selective removal of fines produces a narrower crystal size distribution and higher product purity than FC.

Best for:Fertilizers (ammonium nitrate, potassium chloride), specialty chemicals, applications requiring tight PSD
3

Oslo-Type Crystallizer

Feed enters below a fluidized bed of growing crystals. The upward flow velocity is set to just fluidize the target crystal size, allowing larger crystals to settle and grow while fines are carried up into the supersaturation zone. Produces the largest, most uniform crystals of the three types.

Best for:Large uniform crystals, sugar, potassium nitrate, pharmaceutical intermediates

Which Crystallizer Type to Choose

High throughput (>5 t/h) with broad acceptable CSD

Forced Circulation (FC) — lowest capital cost, most robust, wide application range.

Tight CSD required (fertilizer, chemical salt)

DTB crystallizer — fines removal system gives narrow size distribution with continuous operation.

Largest possible crystals required (sugar, pharmaceutical)

Oslo-type crystallizer — fluidized bed growth mechanism produces the largest, most uniform crystals.

When NOT to Use a Crystallizer

Feed is a slurry that cannot be made supersaturated (non-crystallizable)

Consider instead:Evaporator

Not sure which dryer is right for your process? We'll review your specifications and recommend the optimal solution.

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Frequently Asked Questions — Crystallizers

We need: (1) solute and solvent identity and concentration, (2) required crystal size range (D50 and span or PSD specification), (3) required throughput in t/h of crystalline product, (4) operating temperature and pressure, (5) whether continuous or batch operation is required, (6) any corrosion constraints (material of construction preferences), (7) upstream process (evaporator, reactor, etc.) and downstream requirements (filtration, drying). Send this to info@lozzarprocess.com and we will respond with a preliminary configuration recommendation within 5 business days.

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Request a Quote for This Equipment

Include in your enquiry:

  • Solute name and molecular formula
  • Solvent identity (water, organic solvent)
  • Feed concentration and target product purity
  • Required crystal size (D50 or PSD specification)
  • Required throughput — crystalline product (t/h)
  • Operating temperature and pressure
  • Continuous or batch operation
  • Material of construction preference (SS 316L, Hastelloy, etc.)